Hi David,

thanks for the hint about carbon, didn't know that. That the furnace is top-loading is something I just overlooked. However, the same company has front-loading furnaces and it seems that with the Quikmelt, only the crucible is made out of graphite, the furnace itself doesn't seem to have any. (To be more exact, the description of the Quikmelt says something about organic binder and I'm not sure if that leaks any carbon; the description of the Rapidfire doesn't say anything like that but the material looks similar).

https://www.tabletopfurnace.com/product/rapidfire-pro-l/
https://www.tabletopfurnace.com/product/rapidfire-pro-lp/

The -LP variant has more sophisticated temperature control.

There is another thing that came to my mind about the furnace though: Do they have to be airtight, or placed inside an airtight container, for the doping steps? IIRC doping has to happen under nitrogen or nitrogen/hydrogen atmosphere (or even vacuum) so it doesn't accidentally grow oxide on the silicon.

Greetings,
Martin



On Mon, Apr 12, 2021 at 4:27 PM David Lanzendörfer <leviathan@libresilicon.com> wrote:
Hi
There's a problem... It's for vertical loading and the carbon will contaminate
the circuit. I know those furnaces well, it's used in recycling Aluminum and
for casting. I wanna make a "Liberator" (3D printed gun) into metal
using one of those already for a while.
However, those furnaces are unsuitable for chip making I'm afraid.

Cheers
-lev

On Monday, April 12, 2021 10:49:52 AM WEST Martin Geisse wrote:
> Hi,
>
> so here's some more thoughts about the glove box:
>
> - furnace
>
> I found this mini furnace manufacturer: https://www.tabletopfurnace.com/
>
> They are somewhat outside our price range, about $500, but otherwise they
> match quite well, e.g. https://www.tabletopfurnace.com/product/quikmelt-10/
>
> That furnace is electrically powered (you probably shouldn't use a propane
> furnace indoors), it's tiny so less heat is wasted, and due to its size it
> should be possible to attach it to the back side of the glove box. I still
> think that having the furnace inside the box is a problem because the heat
> cannot escape well, but having it outside and connecting it through another
> opening in the box should be possible.
>
> - insulation
>
> You'll still probably have to thermically insulate the furnace from the
> glove box (even if the back wall is made of sheet metal and not acrylic).
> My first idea is to use calcium silicate boards, e.g.
> https://www.promat.com/en/industry/technologies/calcium-silicates/high-tempe
> rature-insulation/
>
> These boards are used to insulate masonry heaters from walls and can take
> up to 1000°C -- the outside of the furnace is probably not as hot, so that
> should be enough. My guess is to use high-temperature mortar to glue the
> boards to the furnace (keeping the inside dust-free, it's a clean room
> after all) and something more flexible, e.g. high-temperature silicone, to
> glue the boards to the back side of the glove box. If both connections were
> rigid then it would break too easily, especially with thermal expansion.
>
> The alternative would be rock wool, but that stuff is nasty (at least if
> it's similar to glass wool). Calcium silicate is similar to gypsum in
> handling, just more expensive.
>
> - spin coater
>
> My first idea to make this cheap is an axle connected to a disk and mounted
> in such a way that the axle can spin but not tilt. You could then attach a
> handheld drill to the bottom of the axle to spin it.I still like the idea
> except that the disk has to be inside the glove box and the axle has to
> leave the box at the bottom, so keeping it dust-tight AND freely spinnable
> but not tiltable is the main challenge with that. Someone who is wiser in
> mechanics can probably do that easily.
>
>
> Greetings,
> Martin
>
>
>
>
>
> On Sun, Apr 11, 2021 at 12:24 PM David Lanzendörfer <
>
> leviathan@libresilicon.com> wrote:
> > Hi
> > Maybe you can join today 6pm UTC on our Mumble server
> > murmur.libresilicon.com
> > and we can discuss where to best place the airlock and how to build it the
> > easiest and cheapest way?
> >
> > Cheers
> > -lev
> >
> > On Sunday, April 11, 2021 8:17:01 AM WEST Martin Geisse wrote:
> > > Hi David,
> > >
> > > some ideas / questions:
> > > > I was thinking about using sheet metal for everything
> > >
> > > Pardon my ignorance, but how are you going to see what you are doing in
> > > there? Did you mean that one side is still acrylic? Front or top?
> > >
> > > > airlock
> > >
> > > If this is on the side wall, then it is probably hard to reach with your
> > > hands. On the other hand, the back wall (opposite of the gloves) is the
> > > most precious space you have and "wasting" it for the airlock is not
> > > good
> > > either...
> > >
> > > A quick idea would be to attach the airlock at the bottom, with the
> > > outer
> > > door facing towards you and the inner door being a "trap door" in the
> > > bottom of the box.
> > >
> > > > tools
> > >
> > > If everything happens inside the box, space is even more precious.
> > > You'll
> > > need storage for the materials and chemicals, illumination stage, hot
> > > plate, spin coater, furnace, ... A rotating shelf on the back side might
> >
> > be
> >
> > > a solution for that.
> > >
> > > OTOH, an unsolved problem is be what the residual heat of the furnace is
> > > going to do to the acrylic box...
> > >
> > > > gloves
> > >
> > > Gloves always bring the danger of trapping hazardous chemicals *inside*,
> > > right next to your hands. You'll probably need a material that
> > > withstands
> > > *all* of those chemicals, otherwise you might have the piranha etch make
> > > the gloves porous and then HF leak through them... A simple warning not
> >
> > to
> >
> > > spill anything over the gloves is probably not enough because these
> >
> > things
> >
> > > just happen anyway.
> > >
> > > Greetings,
> > > Martin
> > >
> > >
> > >
> > > On Sat, Apr 10, 2021 at 11:33 PM David Lanzendörfer <
> > >
> > > leviathan@libresilicon.com> wrote:
> > > > Hi
> > > > I was thinking about using sheet metal for everything which doesn't
> >
> > need
> >
> > > > to be
> > > > transparent (even cheaper than acrylic glas).
> > > > For the airlock I was figuring I could do a cut out like in the
> >
> > attached
> >
> > > > screen and fold it, then either weld or screw an aluminum box made
> > > > from
> > > > folded
> > > > sheet metal as well.
> > > >
> > > > What do you think?
> > > >
> > > > Cheers
> > > > -lev_______________________________________________
> > > > Libresilicon-developers mailing list
> > > > Libresilicon-developers@list.libresilicon.com
> > > > https://list.libresilicon.com/mailman/listinfo/libresilicon-developers